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1st November 2017 @ 14:12
VTM006 23/10/2017 [data]21278[/data]   VTM004 (0.063 g, 0.146 mmol) was dissolved in toluene (2 mL). Pyrrolidine (0.012 g, 0.175 mmol), CsCO3 (0.066 g, 0.204 mmol), BINAP (4 mg, 6.6 µmol) and Pd (OAc) 2 (0.98 mg, 4.4 µmol) were added in this order to the solution and the mixture was heated at 80 °C for 16 hours. The temperature was increased to 100 °C and the reaction left to stir for two weeks.
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