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17th October 2017 @ 09:43

VTM002                                                                                                                       09/10/2017

VTM002.jpg

4-bromobenzaldehyde (2.02 g, 10.9 mmol) was added to a solution of 2-chloro-6-hydrazineylpyrazine (1.60 g, 11.1 mmol) in EtOH (35 mL) and stirred at room temperature for 16 hours. TLC

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VTM002TLC2.jpg
suggested reaction completion. The mixture was filtered and washed with EtOH (10 mL). The light beige solid was collected (2.23 g, 66 %)

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Attached Files
VTM002.jpg
VTM002TLC.jpg
VTM002TLC2.jpg
VTM002NMR.jpeg