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12th March 2015 @ 20:43

Resynthesis of SGS 4-1. 

SGS 1-2 (crude, 1.007 g, 7.1 mmol) was stirred into MeCN (12 ml). 3-Pyridinecarboxaldehyde (0.74 g, 6.9 mmol, density 1.137 g/mL) was added and the reaction mixture (light brown suspension) was observed. The reaction mixture was stirred at room temperature for 7 days. 

TLC

TLC