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7th May 2015 @ 22:50

7th-8th May 2015

Molecular formula: 

Procedure:

SGS 3-1 (0.164 g, 0.702 mmol) was dissolved in DCM (10 mL) and stirred with PIDA (0.2238 g, 0.695 mmol) overnight.  Solvent was removed in vacuo

After 24 hours, the solution had turned deep red and an initial TLC was conducted in DCM, and a subsequent TLC was then run in EtOAc with 3% MeOH (Rf = 0.33).  

Conducted by Jason Chami, Evan Hockings, James Kalas, James Manton-Hall, Andreas Orsmond, Mackenzie Shaw and Alex Su.

InChI=1S/C10H6ClN5/c11-8-5-13-6-9-14-15-10(16(8)9)7-2-1-3-12-4-7/h1-6H

 

TLC