All Notebooks | Help | Support | About
23rd July 2015 @ 07:16
SSP-3 original composition was a brown liquid. Solvent was evaporated and TLC was performed under various conditions to determine the eluent with the best seperating ability. An 8:2 ethyl acetate: petroleum eluent was used to run SSP-3 in a silica column (25g). A TLC in 8:2 ethyl acetate: petroleum was perfomed to determine fractions which contained the desired product, which were combined into a flask. The solvent was then evaporated under vacuum. The final product yield was 126mg and had a beige, solid appearance.   Strings: SMILES: ClC1=CC=CC(C2=NN=C3C=NC=C(OCCC4=CC=CC=C4)N32)=C1 InChl: InChI=1S/C19H15ClN4O/c20-16-8-4-7-15(11-16)19-23-22-17-12-21-13-18(24(17)19)25-10-9-14-5-2-1-3-6-14/h1-8,11-13H,9-10H2
Attached Files