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24th October 2013 @ 10:46

 

To a well stirred solution of AEW DS 2-1 (100 mg, 0.39 mmol), CH2Cl2 (3 mL) and PhI(OAc)2 (125 mg, 1.94 mmol) was added and the resulting reaction mixture was stirred at room temperature for 48h. An NMR of the solution was taken.

40ml dichloromethane, 5ml methanol and 40ml sodium bicarbonate were added to the resulting mixture, and the layers seperated. The product was then dried using magnesium sulphate, which was removed via vacuum filtration, and the resulting solution was dried under vaccum. An NMR of the remaining solid was taken.

Data:

3ORProject10_DS3-1_241013_1H_bi600.tar

Hazard and Risk Assessment:

Risk Assessment

NMR:

NMR DS 3-1.pdf

 

 

Attached Files
Risk Assessment
NMR DS 3-1.pdf
3ORProject10_DS3-1_241013_1H_bi600.tar