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21st October 2013 @ 09:13

DS 1-1 (1.23 g, 13.2 mmol) was sirred in AcOH (0.41 mL) in MeCN (12.29 mL) and 4-formylbenzonitrile (1.11 g, 13.2 mmol) was added to the orange suspension and the resulting reaction mixture stirred at room temperature for 2 h. The solvent was removed under vacuo to yield an orange/brown solid (XX g, 15.7 mmol, XX% crude yield).

 

TLC (30% EtOAc in Hexane and 100% EtOAc, under UV)

 

TLC 2-1

1H NMR

 

Hazard and Risk Assessment:

Risk Assessment

 

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Risk Assessment
TLC 2-1