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15th August 2016 @ 01:13

N.B. started Sat 13th August: problem with internet connection

 

Procedure:

Crude AEW 305-1(~2.01 mmol, 1 equiv.) was suspended in CH2Cl2 (20 mL) and PhI(OAc)2 (647 mg, 2.01 mmol, 1 equiv.) was added. The reaction mixture was stirred at rt.

 

Strings

InChI=1S/C19H13ClF3N5O2/c20-14-7-12(3-6-15(14)21)26-18(29)16-9-24-10-17(27-16)28-25-8-11-1-4-13(5-2-11)30-19(22)23/h1-10,19H,(H,26,29)(H,27,28)/b25-8+

to

InChI=1S/C19H11ClF3N5O2/c20-13-7-11(3-6-14(13)21)25-18(29)15-8-24-9-16-26-27-17(28(15)16)10-1-4-12(5-2-10)30-19(22)23/h1-9,19H,(H,25,29)

O=C(NC1=CC=C(F)C(Cl)=C1)C2=NC(N/N=C/C3=CC=C(OC(F)F)C=C3)=CN=C2

to

FC(F)OC(C=C1)=CC=C1C2=NN=C3N2C(C(NC4=CC=C(F)C(Cl)=C4)=O)=CN=C3

Attached Files
AEW 307-1.cdxml
AEW 307-1.png