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12th November 2014 @ 04:48

Crude from:

Using modified procedure from:

Resynthesis of JU 2-4:

Reaction performed by Will Talbot and Hugh Russell.




1.36 g of crude SGS 1-1 was stirred into MeCN (12 mL) along with 4-formylbenzonitrile (1.00 g). Glacial AcOH (0.45 mL) was added and the mixture (a light brown suspension) was stirred overnight at room temperature.

Attached Files
sgs 2-1.gif