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14th August 2014 @ 06:15

scheme

TM 43 (pure: from Synthesis of (E)-N-(3-chlorophenyl)-6-(2-(pyridin-3-ylmethylene)hydrazinyl)pyrazine-2-carboxamide (TM 43-1), 100 mg, 0.28 mmol) was stirred into DCM (5 mL), phenyliodine diacetate (PIDA) (1 eq, 0.28 mmol, 90 mg) added, and the reaction mixture stirred at RT for 6 hours.

 

InChIs:

InChI=1S/C17H13ClN6O/c18-13-4-1-5-14(7-13)22-17(25)15-10-20-11-16(23-15)24-21-9-12-3-2-6-19-8-12/h1-11H,(H,22,25)(H,23,24)/b21-9+

to

InChI=1S/C17H11ClN6O/c18-12-4-1-5-13(7-12)21-17(25)14-9-20-10-15-22-23-16(24(14)15)11-3-2-6-19-8-11/h1-10H,(H,21,25)

HIRAC

HIRAC.pdf
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HIRAC.pdf