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11th June 2013 @ 05:06

See also: Hydrolysis of Ethyl 1-(4-fluorophenyl)-2,5-dimethyl-1H-pyrrole-3-carboxylate (AEW 10-1)  

Procedure:

AEW 7-3 (12. 5 g, 48.0 mmol, 1 equiv.) was dissolved in EtOH (120 mL) and 20% NaOH (80 mL, approx 8.5 equiv.). Heated to reflux for x hours.

Reaction was allowed to cool to room temperature then in ice. Acidified (pH 1) with 2M HCl and then cooled in an ice bath for 30 minutes. 

Data:

Hazard and Risk Assessment:

See Hydrolysis of Ethyl 1-(4-fluorophenyl)-2,5-dimethyl-1H-pyrrole-3-carboxylate (AEW 10-1)

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