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6th December 2012 @ 22:18
Mnr: MNR61-70
doi:10.3184/030823409X393628

MNR67_scheme.png
MNR67-3_table.PNG

Hazard Assessment
MNR67-1.pdf


Procedure
To a solution of MNR66-1 (recovered from MNR67-1)(0.260 g, 1.29 mmol) in dioxane (3 mL) was added a 4-fluoroanilne (0.12 mL, 1.29 mmol) and Yb(OTf)3 (0.08 g, 0.13 mmol) the resulting mixture was heated to reflux for 3 hours. The reaction mixture was allowed to cool to room temperature.

TLC of the reaction mixture at this time showed very little, if any, conversion, of the 4-fluoroanilne.
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Attached Files
MNR67-3_table.PNG
MNR67-3_table.PNG