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6th December 2012 @ 21:53
Mnr: MNR61-70
Reaction carried out using the early fraction of MNR66-1 that looked like a furan but did not have the same NMR as the major fractions.

MNR67_scheme.png
MNR67-2_table.PNG

Hazard Assessment
MNR67-1.pdf


Procedure
To a solution of MNR66-1 (0.110 g, 0.54 mmol) in acetic acid (4 mL) was added a 4-fluoroanilne (0.03 mL, 0.36 mmol) and the resulting
mixture was heated to reflux for 3 hours. The reaction mixture was allowed to cool to room temperature.

At this stage, the column for MNR67-1 had been run and had shown no conversion to the desired product.
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Attached Files
MNR67-2_table.PNG
MNR67-2_table.PNG