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Show/Hide Keys
Mnr: MNR51-60
See - Synthesis on JRC13-4
- Synthesis on JRC17-2


Hazard Assessment
Procedure
reaction on at 1600pm 21/11/12
JRC13-4 (0.1 g, 0.586 mmol) was dissolved in methanol (7 mL) and stirred at rt. To the stirring solution was added 2methylindole(0.115 g, 0.88 mmol). The resultant solution was stirred at rt for XX hours.
The reaction was then concentrated and extract xtracted with EtOAc (10 mL), washed with water (2 x 10 mL), organic dried over MgSO4 to yield a XXX
Frac 36-51 - 0.063 g, not SM or product
NMR
Fraction 21-30 - Starting material
Fraction 36-51 - Major spot
JRC15-4
See - Synthesis on JRC13-4
- Synthesis on JRC17-2

Hazard Assessment
HIRAC MNR58.pdf
Procedure
reaction on at 1600pm 21/11/12
JRC13-4 (0.1 g, 0.586 mmol) was dissolved in methanol (7 mL) and stirred at rt. To the stirring solution was added 2methylindole(0.115 g, 0.88 mmol). The resultant solution was stirred at rt for XX hours.
The reaction was then concentrated and extract xtracted with EtOAc (10 mL), washed with water (2 x 10 mL), organic dried over MgSO4 to yield a XXX
Frac 36-51 - 0.063 g, not SM or product
NMR
Fraction 21-30 - Starting material
mnr60-1_frac21-30_1H.pdf
Fraction 36-51 - Major spot
mnr60-1_frac36-51_conc_1H.pdf
mnr60-1_frac36-51_conc_13C.pdf
mnr60-1_frac36-51_conc.zip
JRC15-4
JRC15-4_1H.pdf
JRC15-4_13C.pdf
JRC15-4_conc.zip
Attached Files
Mnr: MNR51-60
See - Synthesis on JRC13-4
- Synthesis on JRC17-2


Hazard Assessment
Procedure
reaction on at 1600pm 21/11/12
JRC13-4 (0.1 g, 0.586 mmol) was dissolved in methanol (7 mL) and stirred at rt. To the stirring solution was added 2,5-dimethylpyrrole(0.09 mL, 0.88 mmol) dropwise. The resultant solution was stirred at rt for XX hours.
The reaction was then concentrated and extract xtracted with EtOAc (10 mL), washed with water (2 x 10 mL), organic dried over MgSO4 to yield a XXX
See - Synthesis on JRC13-4
- Synthesis on JRC17-2

Hazard Assessment
HIRAC MNR58.pdf
Procedure
reaction on at 1600pm 21/11/12
JRC13-4 (0.1 g, 0.586 mmol) was dissolved in methanol (7 mL) and stirred at rt. To the stirring solution was added 2,5-dimethylpyrrole(0.09 mL, 0.88 mmol) dropwise. The resultant solution was stirred at rt for XX hours.
The reaction was then concentrated and extract xtracted with EtOAc (10 mL), washed with water (2 x 10 mL), organic dried over MgSO4 to yield a XXX
Attached Files
Mnr: MNR51-60
See - Synthesis on JRC13-4
- Synthesis on JRC17-2


Hazard Assessment
Procedure
reaction on at 1600pm 21/11/12
JRC13-4 (0.1 g, 0.586 mmol) was dissolved in methanol (7 mL) and stirred at rt. To the stirring solution was added pyrrole (0.061 mL, 0.88 mmol) dropwise. The resultant solution was stirred at rt for XX hours.
The reaction was then concentrated and extract xtracted with EtOAc (10 mL), washed with water (2 x 10 mL), organic dried over MgSO4 to yield a XXX
Frac 8-11 0.029 g - SM
Frac 26-50 0.062 g - not product, not SM
NMR
Fraction 8-11 - Starting material
Fraction 26-50 - Major spot
See - Synthesis on JRC13-4
- Synthesis on JRC17-2

Hazard Assessment
HIRAC MNR58.pdf
Procedure
reaction on at 1600pm 21/11/12
JRC13-4 (0.1 g, 0.586 mmol) was dissolved in methanol (7 mL) and stirred at rt. To the stirring solution was added pyrrole (0.061 mL, 0.88 mmol) dropwise. The resultant solution was stirred at rt for XX hours.
The reaction was then concentrated and extract xtracted with EtOAc (10 mL), washed with water (2 x 10 mL), organic dried over MgSO4 to yield a XXX
Frac 8-11 0.029 g - SM
Frac 26-50 0.062 g - not product, not SM
NMR
Fraction 8-11 - Starting material
mnr58-1_frac8-11_13C.pdf
mnr58-1_frac8-11_1H.pdf
mnr58-1_frac8-11_conc.zip
Fraction 26-50 - Major spot
mnr58-1_frac26-50_1H.pdf
mnr58-1_frac26-50_conc.zip
Attached Files