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1st July 2013 @ 02:19

Reaction Scheme


Procedure:

AEW 58-1 (270 mg, 1.21 mmol) was dissolved in THF (24 mL) and cooled to –78 ˚C. To the stirring solution was added n-BuLi (2.5 M in hexanes, 0.73 mL, 1.82 mmol) and the stirring was continued for 30 minutes. Bromine (0.12 mL, 2.43 mmol) was added dropwise and the reaction mixture was allowed to reach room temperature and stirred for

Data:

 

Hazard and Risk Assessment:


Attached Files
HIRAC AEW 66-1.pdf
AEW 66-1 grid.png
AEW 66-1.png