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2nd July 2014 @ 13:41

Posted in wrong place, moved to Triazolopyrazine Blog: http://malaria.ourexperiment.org/uri/647

GitHub Tag: Issue #

AEW 103-5 (500 mg, 2.48 mmol, 1 equiv.) was dissolved in DMF (3 mL) under Ar. Imidazole (220 mg, 6.18 mmol, 2.5 equiv.) was added and the reaction mixture was stirred at room temperature for 10 minutes. TBS-Cl (484 mg, 3.42 mmol, 1.3 equiv.) was then added and the reaction stirred at room temperature overnight. 

Data:

 

Hazard and Risk Assessment:

 

InChi

InChI=1S/C9H8F2O3/c1-14-9(13)8(12)5-2-3-6(10)7(11)4-5/h2-4,8,12H,1H3

to

InChI=1S/C15H22F2O3Si/c1-15(2,3)21(5,6)20-13(14(18)19-4)10-7-8-11(16)12(17)9-10/h7-9,13H,1-6H3