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1st November 2017 @ 14:12

VTM006

23/10/2017

VTM006.jpg

 

VTM004 (0.063 g, 0.146 mmol) was dissolved in toluene (2 mL). Pyrrolidine (0.012 g, 0.175 mmol), CsCO3 (0.066 g, 0.204 mmol), BINAP (4 mg, 6.6 µmol) and Pd (OAc) 2 (0.98 mg, 4.4 µmol) were added in this order to the solution and the mixture was heated at 80 °C for 16 hours. The temperature was increased to 100 °C and the reaction left to stir for two weeks.

Attached Files
VTM006.jpg