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4th April 2014 @ 00:34

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Exact repeat of Repeat synthesis of methyl pyrazine-2-carboxylate (TM 2-2). Methanol reflux contined for ~36 hours (longer than previously). Yield: 17.8 g, 107 %. Likely due to remaining methanol: the product was obtained as large solid chunks, and so didn't dry particularly well under vacuum.

 

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Re: Repeat synthesis of methyl pyrazine-2-carboxylate (TM 2-3) by Alice Williamson
30th April 2014 @ 06:04
HIRAC seen and approved.