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10th March 2014 @ 06:57

AEW 85-3 (1.91 g, 13.2 mmol) was sirred in AcOH (0.64 mL) in MeCN (19.2 mL) and 4-formylbenzonitrile (1.73 g, 13.2 mmol) was added to the orange suspension and the resulting reaction mixture stirred at room temperature for x h.

TLC (30% EtOAc in Hexane and 100% EtOAc, under UV then stained with ninhydrin)

Hazard and Risk Assessment:

HIRAC AEW 95-2.pdf

InChi:

InChI=1S/C4H5ClN4/c5-3-1-7-2-4(8-3)9-6/h1-2H,6H2,(H,8,9)

and

InChI=1S/C8H5NO/c9-5-7-1-3-8(6-10)4-2-7/h1-4,6H

to

InChI=1S/C12H8ClN5/c13-11-7-15-8-12(17-11)18-16-6-10-3-1-9(5-14)2-4-10/h1-4,6-8H,(H,17,18)/b16-6+

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