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4th December 2013 @ 05:53

 

Crude AEW 102-1 black mixture was dissolved in MeOH (2 mL) and a few drops of H2SO4 was added and the reaction mixture stirred at 80 ˚C for 14 hours.

Data:

TLC (30% EtOAc in hexane)

1H NMR (300 MHz):

 

Ref NMR from CRO:

Methyl ESTER NMR.pdf

 

Hazard and Risk Assessment:

HIRAC AEW 103-1.pdf

InChi:

InChI=1S/C8H6F2O3/c9-5-2-1-4(3-6(5)10)7(11)8(12)13/h1-3,7,11H,(H,12,13)

to

InChI=1S/C9H8F2O3/c1-14-9(13)8(12)5-2-3-6(10)7(11)4-5/h2-4,8,12H,1H3

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