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29th August 2014 @ 03:14

55-1 scheme

 

TM 52 (pure, 170 mg, 0.393 mmol: Synthesis of (E)-N-(3-chlorophenyl)-6-(2-(4-(trifluoromethoxy)benzylidene)hydrazinyl)pyrazine-2-carboxamide (TM 52-1)) was stirred into DCM (6 mL), PIDA (130 mg, 0.393 mmol, 1 eq) added, and the reaction mixture stirred at rt for ?? h.

 

InChIs:

InChI=1S/C19H13ClF3N5O2/c20-13-2-1-3-14(8-13)26-18(29)16-10-24-11-17(27-16)28-25-9-12-4-6-15(7-5-12)30-19(21,22)23/h1-11H,(H,26,29)(H,27,28)/b25-9+

to

InChI=1S/C19H11ClF3N5O2/c20-12-2-1-3-13(8-12)25-18(29)15-9-24-10-16-26-27-17(28(15)16)11-4-6-14(7-5-11)30-19(21,22)23/h1-10H,(H,25,29)

HIRAC:

HIRAC.pdf
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HIRAC.pdf