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29th August 2014 @ 01:36

54 scheme

 

TM 51 (pure, 150 mg, 0.393 mmol: Synthesis of (E)-N-(3-chlorophenyl)-6-(2-(4-methoxybenzylidene)hydrazinyl)pyrazine-2-carboxamide (TM 51-1)) was stirred into DCM (6 mL), PIDA (130 mg, 0.393 mmol, 1 eq) added, and the reaction mixture stirred at rt for ?? g.

InChIs:

InChI=1S/C19H16ClN5O2/c1-27-16-7-5-13(6-8-16)10-22-25-18-12-21-11-17(24-18)19(26)23-15-4-2-3-14(20)9-15/h2-12H,1H3,(H,23,26)(H,24,25)/b22-10+

to

InChI=1S/C19H14ClN5O2/c1-27-15-7-5-12(6-8-15)18-24-23-17-11-21-10-16(25(17)18)19(26)22-14-4-2-3-13(20)9-14/h2-11H,1H3,(H,22,26)

 

HIRAC:

54 HIRAC.pdf
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54 HIRAC.pdf