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14th August 2014 @ 05:56

scheme

TM 42-1 (Pure: from Synthesis of (E)-N-(3-chlorophenyl)-6-(2-(pyridin-2-ylmethylene)hydrazinyl)pyrazine-2-carboxamide (TM 42-1), 100 mg, 0.28 mmol) was stirred into DCM (5 mL), phenyliodine diacetate (PIDA) (1 eq, 0.28 mmol, 90 mg) added, and the reaction mixture stirred at RT for 6 hours.

 

InChIs:

InChI=1S/C17H13ClN6O/c18-12-4-3-6-13(8-12)22-17(25)15-10-19-11-16(23-15)24-21-9-14-5-1-2-7-20-14/h1-11H,(H,22,25)(H,23,24)/b21-9+

to

InChI=1S/C17H11ClN6O/c18-11-4-3-5-12(8-11)21-17(25)14-9-19-10-15-22-23-16(24(14)15)13-6-1-2-7-20-13/h1-10H,(H,21,25)

HIRAC:

HIRAC.pdf

 

 

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scheme.png
HIRAC.pdf