All Notebooks | Help | Support | About
10th December 2016 @ 05:28
New: New

Reaction run on 12/8/16

CC1=NC(C)=C(N=C1Cl)N/N=C/C2=CC=C(OC(F)F)C=C2

Procedure:

4-(difluoromethoxy) benzaldehyde (1.5 mL) was added to 2-chloro-6-hydrazineyl-3,5-dimethylpyrazine (0.8g) in a 50 mL round bottom flask. Ethanol (20 mL) was added to the flask with vigorous stirring. The honey mustard product was left overnight at room temperature. TLC was run on the product to determine completion and presence of desired product. The product was then vacuum filtered resulting in 1.4g of a dried yellow powder. Yield: 1.4/1.10 = 127%


Attached Files
Screen Shot 2016-12-16 at 9.46.10 PM.png
Screen Shot 2016-12-16 at 9.45.56 PM.png