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1st April 2013 @ 22:30

Synthesis for more substrate.

The reaction was performed four times, each with 0.300 g starting material (AT-5) in 8 mL NH3/isopropanol (1:1). The crude was combined and purified by flash column chromatography (95:4.5:0.5 dichloromethane:methanol:ammonia) to give the product as a white solid.

 

NMR

AT-6-1H.pdf
1H NMR

AT-6-13C.pdf
13C{1H} NMR
Linked Posts
Attached Files
AT-6-1.pdf
AT-6-5.jpg
AT-6-1H.pdf
AT-6-13C.pdf